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Figure 17.5. Two-way message exchange between pair of nodes. T2 and T3 are measured in node B s clock while T1 and T4 are measured in node A s clock. (Adapted from reference 12.)

bus. Here, the platform-speci c code lies in the controller extension rather than the media driver, and so it is normally the controller that registers for such drives. In this situation, there could be multiple media drivers associated with that controller, each supporting a different type of removable memory card. For example, a platform including the SD card controller may contain drivers for both the user and protected area SD card sections. The following table lists the possible media IDs. The association between ID and media device family can vary between platforms. What is essential is that each media family supported on the platform has a unique ID. However, the most common media types supported on Symbian OS have acquired default IDs which are shown in the table: Local media ID EFixedMedia0 EFixedMedia1 EFixedMedia2 EFixedMedia3 EFixedMedia4 EFixedMedia5 EFixedMedia6 EFixedMedia7 ERemovableMedia0 ERemovableMedia1 ERemovableMedia2 ERemovableMedia3 Default media device family Internal RAM NOR ash NAND ash MultiMediaCard/SD PC card Code Storage Area (SDIO)

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SCHEME 6.5 Preliminary evaluation of using a protected ribose precursor. Reaction conditions: a, (i) acetone, H2SO4; (ii) TBSCl, imidazole, CH2Cl2, 80%; b, Ph3PCH3Br, t-BuOK, THF, 81%, 19:20 3:1 by NMR; c, Dess Martin periodinane, 91% from 19.

that a node at level n can communicate with a node or a set of nodes at level n 1. In the synchronization phase, the child nodes are synchronized to the parent. The synchronization is initiated by the child node, which sends a synchronization packet at time t1 . This is received by the parent at t2 , and an acknowledgment packet is sent in response at time t3 . The values of t2 and t3 will be included in the acknowledgment packet. This packet is received by the child node at time t4 (see Figure 17.5). Knowing these four time values, the child node can calculate its clock offset relative to the parent node as well as propagation delay as follows: (t2 t1 ) (t4 t3 ) 2 (t2 t1 ) + (t4 t3 ) 2

Note that the de nition of media IDs for removable media devices has altered between EKA1 and EKA2. On EKA1, the ID indicates the slot (or socket) number rather than the media device family. Media drivers and the local media LDD are generally built as combined device driver and kernel extension components. Being extensions means that the kernel will call their DLL entry points early in its boot process

(17.1)

chromatography. Consequently, a follow-up oxidation of this mixture with Dess Martin periodinane (DMP) afforded the desired product ketone 21 and, surprisingly, 20 with its hydroxyl unaffected. To the best of our knowledge, this is the rst example of selective oxidation of a secondary alcohol over a primary alcohol with DMP. Due to the silyl migration of this route (Scheme 6.5), a different protecting group was sought. Reaction of 22a with trityl chloride (to 22b) followed by a Wittig reaction afforded high overall yield of 23 from D-ribose (Scheme 6.6). Dess Martin periodinane oxidation of 23 cleanly furnished the desired product 24 (compare to 17 in Scheme 6.4). Grignard reaction of 24 with vinyl magnesium bromide afforded the diene 25 (compare to 16, Scheme 6.4) in high selectivity. With 25 in hand, it was subjected to RCM reaction conditions with 1 mol% of Grubbs rst generation catalyst. This reaction produced the desired 26 (compare to 15, Scheme 6.4). The stereochemistry of C-40 in 26 was determined by a NOESY spectral analysis. With 26 available, the oxidative rearrangement of its tertiary allylic alcohol was investigated. In this direction, with PCC as the oxidizing agent, enone 27 was rapidly formed but in low yield. Since PCC was known to cleave trityl groups, pyridinium dichromate (PDC), a less acidic oxidizing agent, was investigated. This reaction was found to be successful to 27 if conducted under re uxing conditions. Luche reduction of 27 afforded 28 (compare to 9). This stereoselective reduction gave the allylic alcohol possessing the a-hydroxyl con guration because of the concave structure 27, preventing hydride attack from the bottom face. Conversion of 28 into 29 was carried out under Mitsunobu conditions. Compound 29 was easily transformed into 3 following the procedures of Marquez and co-workers.49

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